2,2,2-三甲基苯乙酮合成路线 （共 203 条）
反应条件
1: iodobenzene With ethylene dibromide; lithium chloride; zinc; chloro-trimethyl-silane in tetrahydrofuran T=50°C; 6 h; 2: in tetrahydrofuran T=0°C; 0.0833333 h; 3: pivaloyl chloride in tetrahydrofuran T=-20 - 25°C;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 36 p. 6040 - 6044
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in toluene T=100°C; Suzuki cross-coupling; 12 h;
参考文献
Synlett, , # 12 p. 1851 - 1854
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=0°C; 6 h; Resolution of racemate;
参考文献
Tetrahedron Letters, , vol. 55, # 11 p. 1943 - 1945
反应条件
bis(1,5-cyclooctadiene)nickel (0); ethyldimethylsilane in toluene T=110°C; 14 h; Inert atmosphere; chemoselective reaction;
参考文献
Organic Letters, , vol. 14, # 3 p. 796 - 799
反应条件
tris-(o-tolyl)phosphine; palladium diacetate in toluene T=20°C; 12 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 2 p. 331 - 340
反应条件
tris-(o-tolyl)phosphine; palladium diacetate in toluene T=20°C; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 78, # 2 p. 331 - 340
反应条件
air; potassium tert-butylate in tetrahydrofuran T=24°C;
参考文献
Tetrahedron Letters, , vol. 33, # 36 p. 5205 - 5208
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene 24 h; Ambient temperature; Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 19, # 13-14 p. 2489 - 2500
反应条件
aluminium trichloride in hexane 5 h; Ambient temperature;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 11 p. 1194 - 1196
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 24 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 75, # 6 p. 1333 - 1345
