2,4,6-三甲基苯甲酰氯合成路线 （共 72 条）
反应条件
thionyl chloride 5 h; Heating;
参考文献
Coste, Jacques; Frerot, Eric; Jouin, Patrick
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2437 - 2446
反应条件
1: With AlCl3, aluminium chloride T=24 - 55°C; 2.16667 h; 2: With hydrogenchloride; water T=45°C; 3: With anhydrous iron chloride; water T=50 - 60°C; 1.63333 h;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/12219 A1, 2005 ;
Location in patent: Page/Page column 11 ;
反应条件
1: With AlCl3, aluminium chloride T=40°C; 2.08333 - 2.88333 h; 2: With hydrogenchloride; water T=3°C;
参考文献
WO2005/12219 A1, ;
Page/Page column 9; 10 ;
反应条件
1: diethyl ether 2: thionyl chloride View Scheme
参考文献
Organic Syntheses, , vol. 21, p. 77
反应条件
1: LiAlH4; diethyl ether 2: hydrogen; CO; benzene / 190 °C / Reagens 4: Octacarbonyldikobalt; Reagens 5: CoCO3 View Scheme
参考文献
Wender et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4079,4082
参考文献
Thiessen; Farr
Journal of Organic Chemistry, 1959 , vol. 24, p. 559
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Wender et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4079,4082
Full Text Show Details
Hauser; Van Eenam
Journal of the American Chemical Society, 1957 , vol. 79, p. 5512,5518
反应条件
polymer(resin Amberlyst A-26)-supported tetracarbonylhydridoferrate anion in dichloromethane 1 h; Heating;
参考文献
Cainelli, Gianfranco; Manescalchi, Francesco; Umani-Ronchi, Achille
Journal of Organometallic Chemistry, 1984 , vol. 276, # 2 p. 205 - 208
反应条件
2: dibutyl ether / anschliessendes Behandeln mit verd. wss. Saeure View Scheme
参考文献
Fuson; Bottorff; Speck
Journal of the American Chemical Society, 1942 , vol. 64, p. 1450
Journal of the American Chemical Society, 1944 , vol. 66, p. 2135
反应条件
1: 4 percent Chromat. / HCOONH4 / Ru3(CO)12 / dioxane / 20 h / 160 °C View Scheme
参考文献
Grattan, T. J.; Whitehurst, J. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 11 - 18
