2,4,6-三甲基苯甲酰氯合成路线 (共 72 条)
反应条件
in dichloromethane
T=20°C;
参考文献
Zaramella, Simone; Stroemberg, Roger; Yeheskiely, Esther
European Journal of Organic Chemistry, 2002 , # 15 p. 2633 - 2639
反应条件
in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Lindsey, Jonathan S.; Muthukumaran, Kannan; Duddu, Sharada S.; Muresan, Ana Z.; Youngblood, W. Justin
Patent: US2006/142562 A1, 2006 ;
Location in patent: Page/Page column 7; 19 ;
反应条件
1: LiAlH4; diethyl ether
2: aqueous hydrobromic acid
View Scheme
参考文献
Hauser; Van Eenam
Journal of the American Chemical Society, 1957 , vol. 79, p. 5512,5518
反应条件
triethylamine in toluene
12 h; Heating;
参考文献
Govindan, Meledath; Pinnick, Harold W.
Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 5011 - 5014
参考文献
Cainelli, Gianfranco; Contento, Michele; Manescalchi, Francesco; Plessi, Laura; Panunzio, Mauro
Gazzetta Chimica Italiana, 1983 , vol. 113, # 7/8 p. 523 - 524
参考文献
Fuson; Corse; Rabjohn
Journal of the American Chemical Society, 1941 , vol. 63, p. 2852
参考文献
Fuson; Corse; Rabjohn
Journal of the American Chemical Society, 1941 , vol. 63, p. 2852
反应条件
in diethyl ether; toluene
T=0°C; 72 h; Inert atmosphere;
参考文献
Zhang, Jian; Yang, Nianfa; Yang, Liwen
Molecules, 2012 , vol. 17, # 6 p. 6415 - 6423
反应条件
AgCN in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=80°C; 0.5 h;
参考文献
Takimoto,S. et al.
Bulletin of the Chemical Society of Japan, 1976 , vol. 49, p. 2335 - 2336
参考文献
Newman; Caflisch
Journal of the American Chemical Society, 1958 , vol. 80, p. 862