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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
938-37-4
合成路线
（共 30 条）
6973-60-0
N-甲基-2-吡咯羧酸
+
108-90-7
氯苯
→
反应条件
938-37-4
反应条件
Pd0(tris(tert-butyl)phosphine)2; tetrabutyl-ammonium chloride; caesium carbonate in N,N-dimethyl-formamide T=170°C; 0.133333 h; Microwave irradiation;
参考文献
Bilodeau, Francois; Brochu, Marie-Christine; Guimond, Nicolas; Thesen, Kris H.; Forgione, Pat
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1550 - 1560
6973-60-0
N-甲基-2-吡咯羧酸
+
591-50-4
碘苯
→
反应条件
938-37-4
反应条件
Pd0(tris(tert-butyl)phosphine)2; tetrabutyl-ammonium chloride; caesium carbonate in N,N-dimethyl-formamide T=170°C; 0.133333 h; Microwave irradiation;
参考文献
Bilodeau, Francois; Brochu, Marie-Christine; Guimond, Nicolas; Thesen, Kris H.; Forgione, Pat
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1550 - 1560
6973-60-0
N-甲基-2-吡咯羧酸
+
17763-67-6
苯基三氟甲烷磺酸酯
→
反应条件
938-37-4
反应条件
Pd0(tris(tert-butyl)phosphine)2; tetrabutyl-ammonium chloride; caesium carbonate in N,N-dimethyl-formamide T=170°C; 0.133333 h; Microwave irradiation;
参考文献
Bilodeau, Francois; Brochu, Marie-Christine; Guimond, Nicolas; Thesen, Kris H.; Forgione, Pat
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1550 - 1560
96-54-8
N-甲基吡咯
→
反应条件
938-37-4
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile T=25°C; 12 h; Inert atmosphereIrradiationSchlenk technique;
参考文献
Liu, Yu-Xia; Xue, Dong; Wang, Jia-Di; Zhao, Cong-Jun; Zou, Qing-Zhu; Wang, Chao; Xiao, Jianliang
Synlett, 2013 , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
96-54-8
N-甲基吡咯
+
16668-99-8
→
反应条件
938-37-4
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile T=25°C; 12 h; Inert atmosphereIrradiationSchlenk technique;
参考文献
Liu, Yu-Xia; Xue, Dong; Wang, Jia-Di; Zhao, Cong-Jun; Zou, Qing-Zhu; Wang, Chao; Xiao, Jianliang
Synlett, 2013 , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
96-54-8
N-甲基吡咯
+
1483-73-4
二苯基溴化碘
→
反应条件
938-37-4
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile T=25°C; 12 h; Inert atmosphereIrradiationSchlenk technique;
参考文献
Liu, Yu-Xia; Xue, Dong; Wang, Jia-Di; Zhao, Cong-Jun; Zou, Qing-Zhu; Wang, Chao; Xiao, Jianliang
Synlett, 2013 , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
108-86-1
溴代苯
+
87236-62-2
→
反应条件
938-37-4
反应条件
[1,4-bis-(diphenylphosphine)butane]palladium (II) dichloride in tetrahydrofuran 1 h; Heating;
参考文献
Minato, Akio; Tamao, Kohei; Hayashi, Tamio; Suzuki, Keizo; Kumuda, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 52 p. 5319 - 5322
96-54-8
N-甲基吡咯
+
108-90-7
氯苯
→
反应条件
938-37-4
反应条件
potassium phosphate; palladium diacetate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1-methyl-pyrrolidin-2-one T=15 - 125°C; 24.25 h; Inert atmosphere;
参考文献
Nadres, Enrico T.; Lazareva, Anna; Daugulis, Olafs
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 471 - 483
96-54-8
N-甲基吡咯
+
98-09-9
苯磺酰氯
→
反应条件
938-37-4
反应条件
potassium acetate; palladium diacetate; copper (II) acetate monohydrate in N,N-dimethyl acetamide T=130°C; 24 h; regioselective reaction;
参考文献
Jafarpour, Farnaz; Olia, Mina Barzegar Amiri; Hazrati, Hamideh
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3407 - 3412
75311-50-1
→
反应条件
938-37-4
反应条件
boron trichloride; lithium hexamethyldisilazane in tetrahydrofuran; dichloromethane 24 h; Ambient temperaturefirst 30 min at -78 deg C;
参考文献
Magedov, Igor V.; Kornienko, Alexander V.; Zotova, Tatyana O.; Drozd, Victor N.
Tetrahedron Letters, 1995 , vol. 36, # 26 p. 4619 - 4622
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