4-甲基-3-硝基苯甲腈合成路线 （共 38 条）
反应条件
sulfuric acid; nitric acid T=0°C; 2 h;
参考文献
Allison, Brett D.; Hack, Michael D.; Phuong, Victor K.; Rabinowitz, Michael H.; Rosen, Mark D.
Patent: US2005/38032 A1, 2005 ;
Location in patent: Page/Page column 29 ;
US 20050038032 A1
反应条件
hydroxylamine hydrochloride; iron(II) sulfate in N,N-dimethyl-formamide 3.05 h; Reflux;
参考文献
Patil, Dinanath D.; Wadhava, Gurumeet C.; Deshmukh, Arun K.
Asian Journal of Chemistry, 2012 , vol. 24, # 3 p. 1401 - 1402
反应条件
bis(piperidino)methane; 1,5-bis-(diphenylphosphino)-pentane; palladium diacetate in toluene T=160°C; 16 h;
参考文献
Sundermeier, Mark; Zapf, Alexander; Mutyala, Sateesh; Baumann, Wolfgang; Sans, Juergen; Weiss, Stefan; Beller, Matthias
Chemistry - A European Journal, 2003 , vol. 9, # 8 p. 1828 - 1836
反应条件
copper diacetate; silver(l) oxide in 1-methyl-pyrrolidin-2-one T=120°C; 20 h;
参考文献
Zheng, Kui; Yu, Peng; Chen, Shuyou; Chen, Fen; Cheng, Jiang
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 449 - 452
反应条件
sodium azide; 2-nitropropane sodium salt in dimethyl sulfoxide T=17°C; 0.0305556 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 27 p. 7700 - 7708
反应条件
1: NH4Cl / methanol / 72 h / Ambient temperature 2: 52 percent / NaCl, NaOCl / dimethylsulfoxide; hexane / 3 h / Ambient temperature 3: NaN3, 2-nitropropane sodium salt / dimethylsulfoxide / 0.03 h / 17 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 27 p. 7700 - 7708
反应条件
sodium azide in dimethylsulfoxide-d6 Ambient temperatureIrradiationrelative rate; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 58, # 27 p. 7700 - 7708
反应条件
in methanol T=25°C; Rate constantMechanism;
参考文献
Journal of Organic Chemistry, , vol. 58, # 27 p. 7700 - 7708
参考文献
Chemische Berichte, , vol. 27, p. 2165
