4-甲基-3-硝基苯甲腈合成路线 （共 38 条）
反应条件
1: 90 percent / piperidine / 24 h / 100 °C
2: 34 percent / triethylphosphite / 20 h / Heating
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 54 percent / piperidine / 24 h / 100 °C
2: 53 percent / triethylphosphite / 20 h / Heating
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 99 percent / dimethylformamide / Heating
2: 77 percent / NaIO4 / tetrahydrofuran; H2O / 2.5 h
View Scheme
参考文献
Reich; Lenz
Helvetica Chimica Acta, 1920 , vol. 3, p. 148
反应条件
1: 92 percent / piperidine / 24 h / 100 °C
2: 78 percent / triethylphosphite / 20 h / Heating
3: 2) 2N HCl / 2) 1 h
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 92 percent / piperidine / 24 h / 100 °C
2: 78 percent / triethylphosphite / 20 h / Heating
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 92 percent / piperidine / 24 h / 100 °C
2: 78 percent / triethylphosphite / 20 h / Heating
3: 1) ethanol; 2) NH3 / 1) CHCl3; 2) ethanol
View Scheme
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: aq. Na2Cr2O7, H2SO4
2: N2H4 / Pd-C / ethanol
3: aq. NaHCO3
View Scheme
参考文献
Chan,R.L.; Bruice,T.C.
Journal of the American Chemical Society, 1977 , vol. 99, p. 6721 - 6730
反应条件
1: sulfuric acid / Hydrolysis
2: permanganate; NaOH-solution
3: phosphorus pentachloride / 100 °C
View Scheme
参考文献
Soderman; Johnson
Journal of the American Chemical Society, 1925 , vol. 47, p. 1394
