反应条件
1: LiAlH4, cc. HCl / benzene / 1.) ice-water bath, 30 min 2.) RT, 2.5 h 2.) 0 deg C, 5 min
2: 30.5 g / KHCO3 / 0.42 h / 65 °C
3: 54 percent / 20percent HCl / 52 h / 38 °C
View Scheme
参考文献
Dowd; Shapiro; Kang
Tetrahedron, 1984 , vol. 40, # 16 p. 3069 - 3086
