反应条件
1: 90 percent / aq. NaHCO3 / ethyl acetate 2: N-methylmorpholine / CH2Cl2 / 0.25 h / -5 °C 3: N-methylmorpholine, 2,6-luditine / CH2Cl2; dimethylformamide / 1.) 0 deg C, 1 h, 2.) r. t., 1 h 4: 91 percent / aq. NaOH / dimethylformamide / 6 h 5: 40 percent / aq. HCl / dioxane / 6 h View Scheme
参考文献
Smith, D. David; Boyd, Kenneth G.; Hopton, David; Baxter, Robert L.; Ramage, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 5 p. 551 - 556
