[3-(烯丙基氧基)丙基]苯合成路线 （共 12 条）
反应条件
titanium(IV) isopropylate; magnesium; ethylene dibromide in tetrahydrofuran T=20°C; 11 h;
参考文献
Ohkubo, Mutsumi; Mochizuki, Sayaka; Sano, Takeshi; Kawaguchi, Yuuki; Okamoto, Sentaro
Organic Letters, 2007 , vol. 9, # 5 p. 773 - 776
反应条件
aluminium trichloride; N,N-dimethyl-aniline in dichloromethane 1 h; Heating;
参考文献
Akiyama, Takahiko; Hirofuji, Hajimu; Ozaki, Shoichiro
Tetrahedron Letters, 1991 , vol. 32, # 10 p. 1321 - 1324
反应条件
aluminium trichloride; N,N-dimethyl-aniline in dichloromethane 1 h; Heating;
参考文献
Tetrahedron Letters, , vol. 32, # 10 p. 1321 - 1324
反应条件
triphenylphosphine; palladium diacetate in tetrahydrofuran
Heating;
参考文献
Haight, Anthony R.; Stoner, Eric J.; Peterson, Matthew J.; Grover, Vandana K.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8092 - 8096
反应条件
triethylsilane; iron(III) chloride in nitromethane
T=20°C; 0.166667 h;
参考文献
Iwanami, Katsuyuki; Seo, Hana; Tobita, Yuki; Oriyama, Takeshi
Synthesis, 2005 , # 2 art. no. F12004SS, p. 183 - 186
反应条件
polymethylhydrosiloxane in toluene
T=110°C; Inert atmosphere;
参考文献
Sakai, Norio; Usui, Yuta; Moriya, Toshimitsu; Ikeda, Reiko; Konakahara, Takeo
European Journal of Organic Chemistry, 2012 , # 24 p. 4603 - 4608
反应条件
triphenylphosphine; palladium diacetate in tetrahydrofuran
Heating;
参考文献
Haight, Anthony R.; Stoner, Eric J.; Peterson, Matthew J.; Grover, Vandana K.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8092 - 8096
反应条件
triphenylphosphine; palladium diacetate in tetrahydrofuran
Heating;
参考文献
Haight, Anthony R.; Stoner, Eric J.; Peterson, Matthew J.; Grover, Vandana K.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8092 - 8096
反应条件
1: indium tribromide / toluene / 20 h / 110 °C / |Inert atmosphere
2: polymethylhydrosiloxane / toluene / 110 °C / |Inert atmosphere
View Scheme
参考文献
Sakai, Norio; Usui, Yuta; Moriya, Toshimitsu; Ikeda, Reiko; Konakahara, Takeo
European Journal of Organic Chemistry, 2012 , # 24 p. 4603 - 4608
反应条件
sodium hydride
1.) DMF, 0 deg C, 2.) DMF, 20 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Akiyama, Takahiko; Hirofuji, Hajimu; Ozaki, Shoichiro
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 7 p. 1932 - 1938
