1: aniline With hydrogenchloride; sodium nitrite in water
Diazotization;
2: ethyl 3-oxo-3-phenylpropionate With sodium acetate in ethanol; water
T=0°C; Addition; 2 h; Further stages.;
参考文献
Ishida, Keishi; Murakami, Masahiro
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 5898 - 5900
1.1: water; potassium hydroxide / 24 h / 20 °C
1.2: 0 - 5 °C
2.1: water / 2 h / 0 - 5 °C
3.1: montmorillonite K10 / methanol; water / 2 h / Reflux
4.1: nitrobenzene / 2 h / Reflux
View Scheme
参考文献
Al-Awadi, Nouria A.; Ibrahim, Maher R.; Al-Etaibi, Alya M.; Elnagdi, Mohamed H.
Arkivoc, 2011 , vol. 2011, # 2 p. 310 - 321
