反应条件
1: N-chloro-succinimide; palladium diacetate; sodium peroxodisulphate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 4 h / 70 °C / |Sealed tube
2: N-chloro-succinimide; palladium diacetate; sodium peroxodisulphate; trifluorormethanesulfonic acid / 1,2-dichloro-ethane / 6 h / 60 °C / |Sealed tube
3: potassium hydroxide / methanol / 12 h / |Sealed tube; |Reflux
View Scheme
参考文献
Sun, Xiuyun; Shan, Gang; Sun, Yonghui; Rao, Yu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 16 p. 4440 - 4444
Angew. Chem., 2013 , vol. 125, # 16 p. 4536 - 4540,5