Edginton, Andrea N.; Rouleau, Claude; Stephenson, Gerald R.; Boermans, Herman J.
Archives of Environmental Contamination and Toxicology, 2007 , vol. 52, # 1 p. 113 - 120
1: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
T=20°C; 0.5 h;
2: With sodium tetrahydroborate; water in tetrahydrofuran
T=0°C; 0.5 h;
1: HNO3 / 30 - 40 °C
2: iron (II)-sulfate; aqueous ammonia
3: sulfuric acid / 0 - 5 °C / Diazotization.Erwaermen der Diazoniumsalz-Loesung mit KI auf 70-80grad
View Scheme
参考文献
Wolfe et al.
Journal of Organic Chemistry, 1949 , vol. 14, p. 900
