N-(4-氯苯基)氨基甲酸甲酯合成路线 (共 27 条)
反应条件
1: TolSO2N=IPh / dichloromethane / 1 h / 20 °C / Inert atmosphere
2: dichloromethane / 4.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Yoshimura, Akira; Luedtke, Matthew W.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 2087 - 2091
反应条件
1: carbon monoxide With potassium superoxide; tetrabutylammomium bromide in N,N-dimethyl-formamide
0.25 h;
2: 4-chloro-aniline in N,N-dimethyl-formamide
0.108333 h; Microwave irradiation;
3: methyl iodide in N,N-dimethyl-formamide
参考文献
Singh, Satish Kumar; Verma, Manjusha; Singh, Krishna Nand
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2008 , vol. 47, # 10 p. 1545 - 1548
反应条件
in N,N-dimethyl-formamide
参考文献
Singh, Krishna Nand
Synthetic Communications, 2007 , vol. 37, # 16 p. 2651 - 2654
参考文献
Izawa, Yasuji; Ishiguro, Katsuhiro; Tomioka, Hideo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 951 - 952
反应条件
(i) nBu3SnN3, (ii) /BRN= 1098229/; Multistep reaction;
参考文献
Kricheldorf,R.; Leppert,E.
Synthesis, 1976 , p. 329 - 330
参考文献
Templeman; Sexton
Pr.roy.Soc.<B>, 1946 , vol. 133, p. 480,482
反应条件
in 1,2-dichloro-ethane; toluene
T=-30 - 65°C; 168 h;
参考文献
El Kaim, Laurent; Grimaud, Laurence; Lee, Anabelle; Perroux, Yannick; Tirla, Cornelia
Organic Letters, 2004 , vol. 6, # 3 p. 381 - 383