反应条件
in dichloromethane inert atmosphere; dropwise addn. of 1 equiv. PCl5 to amine at 25°C, stirring for 12 h; not isolated, detd. by (31)P-NMR spectroscopy;
参考文献
Allcock, Harry R.; Crane, Chester A.; Morrissey, Christopher T.; Olshavsky, Michael A.
Inorganic Chemistry, 1999 , vol. 38, # 2 p. 280 - 283