4-(3-乙氧基-2-羟基丙氧基)苯胺合成路线 （共 6 条）
反应条件
iron(III) chloride; hydrazine in methanol Heating;
参考文献
Tamura, Rui; Fujimoto, Daisuke; Lepp, Zsolt; Misaki, Kentaro; Miura, Hideyuki; Takahashi, Hiroki; Ushio, Takanori; Nakai, Tadashi; Hirotsu, Ken
Journal of the American Chemical Society, 2002 , vol. 124, # 44 p. 13139 - 13153
反应条件
1: 89 percent / BnNMe3Cl / toluene / 110 °C 2: 81 percent / NH2NH2; FeCl3 / methanol / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 44 p. 13139 - 13153
反应条件
1: 83 percent / aq. NaOH / 25 °C 2: 89 percent / BnNMe3Cl / toluene / 110 °C 3: 81 percent / NH2NH2; FeCl3 / methanol / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 44 p. 13139 - 13153
反应条件
1: 1.) pyridine, 2.) aq. KOH / 1.) 90 deg C, 6 h, 2.) acetone, RT, 2 h 2: H2SO4 / 6 h / 80 °C 3: H2 / 10percent Pd/C / ethanol / 8 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 18 p. 3330 - 3336
反应条件
1: H2SO4 / 6 h / 80 °C 2: H2 / 10percent Pd/C / ethanol / 8 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 41, # 18 p. 3330 - 3336
反应条件
1: Et3N / CH2Cl2 / 3 h / 10 °C 2: CH2Cl2 / 120 h / Ambient temperature View Scheme
参考文献
Tada, Yukio; Yamawaki, Ichiro; Ueda, Shuichi; Matsumoto, Hiroshi; Matsuura, Naosuke; Yasumoto, Mitsugi; Koda, Akihide; Hori, Mikio
Journal of Medicinal Chemistry, 1998 , vol. 41, # 18 p. 3330 - 3336
