in hexane
react. of excess GeI2 with the butadiene in refluxing n-hexane; methylation of the resulting Ph2C4H4GeI2 with MeMgBr; 1H NMR spectrum, elem. anal., mass spectrum;
参考文献
Koecher, Juergen; Neumann, Wilhelm P.
Organometallics, 1985 , vol. 4, p. 400 - 402
in benzene
Kinetics; at 70-80 °C; competition experiment; excess of both CH2=CPh-CPh=CH2 and CH2=CHPh applied; react. mechanism discussed; 1H NMR spectrum;
参考文献
Koecher, Juergen; Neumann, Wilhelm P.
Organometallics, 1985 , vol. 4, p. 400 - 402