3',5'-二甲氧基苯甲酰苯胺合成路线 （共 7 条）
反应条件
copper(I) oxide; water; caesium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate; sodium hydroxide; N-methyl-2-(methylamino)ethylamine
T=100°C; 12 h; Inert atmosphereSealed tube;
参考文献
Wang, Jichao; Yin, Xinchi; Wu, Jun; Wu, Datong; Pan, Yuanjiang
Tetrahedron, 2013 , vol. 69, # 48 p. 10463 - 10469
反应条件
triethylamine in tetrahydrofuran
T=20°C; 1 h;
参考文献
Hadjeri; Mariotte; Boumendjel
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 10 p. 1352 - 1355
反应条件
1: 3,5-dimethoxybenzenamine With n-butyllithium in hexane
T=20°C; 1 h;
2: benzoyl-protected allyl alcohol in hexane
T=20°C; 12 h;
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
tin(IV) chloride in 1,2-dichloro-ethane
Heating;
参考文献
Hadjeri, Mohamed; Mariotte, Anne-Marie; Boumendjel, Ahcene
Journal of Chemical Research - Part S, 2002 , # 9 p. 463 - 464
反应条件
1.1: 87 percent / thionyl chloride / 0 - 20 °C
2.1: n-butyl lithium / hexane / 1 h / 20 °C
2.2: 65 percent / hexane / 12 h / 20 °C
View Scheme
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
1: aqueous sodium hypobromite / -15 °C
2: potassium carbonate; diethyl ether
View Scheme
参考文献
Seka; Fuchs
Monatshefte fuer Chemie, 1931 , vol. 57, p. 52,58
反应条件
1: liquid ammonia
2: aqueous sodium hypobromite / -15 °C
3: potassium carbonate; diethyl ether
View Scheme
参考文献
Seka; Fuchs
Monatshefte fuer Chemie, 1931 , vol. 57, p. 52,58
