(S)-3-(甲基磺酰氧基)哌啶-1-羧酸叔丁酯合成路线 (共 3 条)
反应条件
in methanol T=90°C; 48 h; Sealed tube;
参考文献
VERTEX PHARMACEUTICALS INCORPORATED
Patent: US2010/137305 A1, 2010 ;
Location in patent: Page/Page column 33 ;
反应条件
sodium hydride in N,N-dimethyl-formamide T=0 - 120°C; Title compound not separated from byproducts.;
参考文献
Synthetic Communications, , vol. 38, # 4 p. 517 - 524
反应条件
sodium hydride in N,N-dimethyl-formamide T=0 - 120°C; Title compound not separated from byproducts.;
参考文献
Synthetic Communications, , vol. 38, # 4 p. 517 - 524