1-苯磺酰基-4-氯-2-碘-7-氮杂吲哚合成路线 （共 4 条）
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran T=-78°C; 0.5 h; 2: With iodine in tetrahydrofuran T=-78°C; 4 h;
参考文献
US2007/129364 A1, ;
Page/Page column 80-81 ;
US 20070129364 A1
反应条件
1: With N,N,N',N,-tetramethylethylenediamine; lithium diisopropyl amide in tetrahydrofuran T=-70°C; 2: With iodine in tetrahydrofuran T=-70°C;
参考文献
Layek, Mohosin; Gajare, Vikas; Kalita, Dipak; Islam, Aminul; Mukkanti; Pal, Manojit
Tetrahedron, 2009 , vol. 65, # 25 p. 4814 - 4819
反应条件
copper(l) iodide; palladium 10 on activated carbon; triethylamine; triphenylphosphine in water T=80°C; Sonogashira coupling; Inert atmosphere; regioselective reaction;
参考文献
Layek, Mohosin; Gajare, Vikas; Kalita, Dipak; Islam, Aminul; Mukkanti; Pal, Manojit
Tetrahedron, 2009 , vol. 65, # 25 p. 4814 - 4819
反应条件
copper(l) iodide; palladium 10 on activated carbon; triethylamine; triphenylphosphine in water T=80°C; Sonogashira coupling; Inert atmosphere; regioselective reaction;
参考文献
Layek, Mohosin; Gajare, Vikas; Kalita, Dipak; Islam, Aminul; Mukkanti; Pal, Manojit
Tetrahedron, 2009 , vol. 65, # 25 p. 4814 - 4819
