3-乙氧基羰基-2-甲基喹噁啉合成路线 （共 7 条）
反应条件
in methanol 2 h; Ambient temperature;
参考文献
Bartoszek, M.; Salzwedel, D.; Stumm, G.; Niclas, H.-J.
Organic Mass Spectrometry, 1987 , vol. 22, p. 259 - 268
反应条件
reduction of Dirlam and McFarland;
参考文献
Bartoszek, M.; Salzwedel, D.; Stumm, G.; Niclas, H.-J.
Organic Mass Spectrometry, 1987 , vol. 22, p. 259 - 268
反应条件
1: 24.2 g / triethylamine / ethanol / 2 h / 40 - 45 °C
2: trimethylphosphite / propan-1-ol / 1.5 h / Heating
View Scheme
参考文献
Li, Jian-Yong; Zhang, Ji-Yu; Zhou, Xu-Zheng; Li, Jin-Shan; Lu, Run-Hua
Heterocyclic Communications, 2007 , vol. 13, # 1 p. 49 - 56
反应条件
1: 32 g / sodium hypochlorite; potassium hydroxide / aq. ethanol / 0 °C
2: 24.2 g / triethylamine / ethanol / 2 h / 40 - 45 °C
3: trimethylphosphite / propan-1-ol / 1.5 h / Heating
View Scheme
参考文献
Li, Jian-Yong; Zhang, Ji-Yu; Zhou, Xu-Zheng; Li, Jin-Shan; Lu, Run-Hua
Heterocyclic Communications, 2007 , vol. 13, # 1 p. 49 - 56
反应条件
sodium dithionite in methanol; water
T=40°C; 6 h;
参考文献
Stumm, Gerhard; Niclas, Hans-Joachim
Zeitschrift fuer Chemie (Stuttgart, Germany), 1989 , vol. 29, # 6 p. 208 - 209
参考文献
Landquist; Silk
Journal of the Chemical Society, 1956 , p. 2052,2055
反应条件
sodium hydroxide
3 h; Heating;
参考文献
Li, Jian-Yong; Zhang, Ji-Yu; Zhou, Xu-Zheng; Li, Jin-Shan; Lu, Run-Hua
Heterocyclic Communications, 2007 , vol. 13, # 1 p. 49 - 56
