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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
941279-81-8
合成路线
（共 16 条）
941279-81-8
→
反应条件
22945-63-7
(2-甲氧基苯基)(2-吡啶基)甲酮
反应条件
1: palladium (II) trifluoroacetate; caesium carbonate; tri-cyclo-hexyl-phosphine / o-xylene; toluene / 6 h / Inert atmosphere; Reflux 2: ferrous chloride tetrahydrate; oxygen; acetic acid / dimethyl sulfoxide / 24 h / 100 °C View Scheme
参考文献
De Houwer, Johan; Abbaspour Tehrani, Kourosch; Maes, Bert U. W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2745 - 2748
941279-81-8
→
反应条件
27693-37-4
2-(3-硝基苯甲酰)吡啶
反应条件
1: palladium (II) trifluoroacetate; caesium carbonate; tri-cyclo-hexyl-phosphine / o-xylene; toluene / 6 h / Inert atmosphere; Reflux 2: copper(l) iodide; oxygen; acetic acid / dimethyl sulfoxide / 24 h / 100 °C View Scheme
参考文献
De Houwer, Johan; Abbaspour Tehrani, Kourosch; Maes, Bert U. W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2745 - 2748
941279-81-8
+
623-12-1
4-氯苯甲醚
→
反应条件
6305-18-6
(4-甲氧基苯基)(吡啶-2-基)甲酮
反应条件
1: palladium (II) trifluoroacetate; caesium carbonate; tri-cyclo-hexyl-phosphine / o-xylene; toluene / 6 h / Inert atmosphere; Reflux 2: ferrous chloride tetrahydrate; oxygen; acetic acid / dimethyl sulfoxide / 24 h / 100 °C View Scheme
参考文献
De Houwer, Johan; Abbaspour Tehrani, Kourosch; Maes, Bert U. W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2745 - 2748
109-09-1
2-氯吡啶
+
941279-81-8
→
反应条件
1132-37-2
二吡啶-2-甲烷
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium (II) trifluoroacetate in toluene; xylene Heating;
参考文献
Niwa, Takashi; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2007 , vol. 46, # 15 p. 2643 - 2645
941279-81-8
+
2398-37-0
间溴苯甲醚
→
反应条件
35854-44-5
2-(3-甲氧基苄基)吡啶
反应条件
palladium (II) trifluoroacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene; toluene 6 h; Inert atmosphereReflux;
参考文献
De Houwer, Johan; Abbaspour Tehrani, Kourosch; Maes, Bert U. W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2745 - 2748
941279-81-8
+
108-90-7
氯苯
→
反应条件
101-82-6
2-苄基吡啶
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium (II) trifluoroacetate in toluene; xylene 6 h; Heating;
参考文献
Niwa, Takashi; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2007 , vol. 46, # 15 p. 2643 - 2645
941279-81-8
+
591-50-4
碘苯
→
反应条件
101-82-6
2-苄基吡啶
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium (II) trifluoroacetate in toluene Heating;
参考文献
Niwa, Takashi; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2007 , vol. 46, # 15 p. 2643 - 2645
941279-81-8
+
108-86-1
溴代苯
→
反应条件
101-82-6
2-苄基吡啶
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium (II) trifluoroacetate in toluene Heating;
参考文献
Niwa, Takashi; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2007 , vol. 46, # 15 p. 2643 - 2645
941279-81-8
+
610-96-8
2-氯苯甲酸甲酯
→
反应条件
7547-92-4
反应条件
palladium (II) trifluoroacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene; toluene 6 h; Inert atmosphereReflux;
参考文献
De Houwer, Johan; Abbaspour Tehrani, Kourosch; Maes, Bert U. W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2745 - 2748
941279-81-8
+
610-96-8
2-氯苯甲酸甲酯
→
反应条件
7547-92-4
+
1374650-41-5
反应条件
palladium (II) trifluoroacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene; toluene 6 h; Inert atmosphereReflux;
参考文献
De Houwer, Johan; Abbaspour Tehrani, Kourosch; Maes, Bert U. W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2745 - 2748
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