1,2,3,4-四氢咔唑合成路线 (共 202 条)
反应条件
diethyl ether; methyllithium; tert.-butyl lithium 1.) THF, pentane, -78 deg C, 1 h; 2.) -10 deg C, 45 min, then ambient temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 39, # 22 p. 3767 - 3776
参考文献
Chemische Berichte, , vol. 26, p. 2006
Gazzetta Chimica Italiana, , vol. 23 II, p. 296
Chemische Berichte, , vol. 40, p. 3227
反应条件
butane-1-thiol in tetrachloromethane T=25°C; Rate constant;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 57, # 8 p. 1826 - 1835,1632 - 1640
反应条件
C22H25ClIrN6O2(1+)*C32H12BF24(1-); potassium hydroxide in deuterated toluene T=110°C; 100 h; Inert atmosphere; Catalytic behavior; Reagent/catalystTimeSolvent;
参考文献
Organometallics, , vol. 31, # 21 p. 7500 - 7510
反应条件
Fremy’s salt; acetone in gepufferter wss. Loesung;
参考文献
Chemische Berichte, , vol. 87, p. 1251,1253
参考文献
Matlin, Stephen A.; Barron, Kenneth
Journal of Chemical Research, Miniprint, 1990 , # 8 p. 1920 - 1943
反应条件
acetic acid 24 h; Ambient temperature;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 22, # 1 p. 38 - 44
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 22, # 1 p. 46 - 52
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 209, p. 317
Bulletin de la Societe Chimique de France, , p. 438,444
反应条件
mercaptoacetic acid in dichloromethane 0.5 h; Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 26, # 2 p. 161 - 164
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 22, # 16 p. 1475 - 1478