1,2,3,4-四氢咔唑合成路线 （共 202 条）
反应条件
titanium(III) chloride; ammonium acetate in acetone T=20°C; 0.25 h;
参考文献
Iwama, Tetsuo; Birman, Vladimir B.; Kozmin, Sergey A.; Rawal, Viresh H.
Organic Letters, 1999 , vol. 1, # 4 p. 673 - 676
反应条件
2-Bromo-1,3,5-trimethyl-benzene; potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=150°C; 2 h;
参考文献
Aoyagi, Yutaka; Shishikura, Masahiro; Mizusaki, Toshihiko; Komine, Takashi; Yoshinaga, Tokuji; Inaba, Haruko; Ohta, Akihiro; Takeya, Koichi
Heterocycles, 2008 , vol. 75, # 5 p. 1055 - 1059
反应条件
carbon monoxide; bis-triphenylphosphine-palladium(II) chloride; tin(ll) chloride in 1,4-dioxane T=100°C; 16 h;
参考文献
Akazome, Motohiro; Kondo, Teruyuki; Watanabe, Yoshihisa
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3375 - 3380
反应条件
1,4-diaza-bicyclo[2.2.2]octane; nitrogen; palladium diacetate in isopropanol acetate; water; cyclohexanone; N,N-dimethyl-formamide
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=110°C; 1.5 h;
参考文献
Zhao, Xiaodan; Yu, Zhengkun; Xu, Tongyu; Wu, Ping; Yu, Haifeng
Organic Letters, 2007 , vol. 9, # 25 p. 5263 - 5266
反应条件
trifluoroacetic acid in dichloromethane 12 h; RefluxInert atmosphere;
参考文献
Barluenga, Jose; Jimenez-Aquino, Agustin; Aznar, Fernando; Valdes, Carlos
Journal of the American Chemical Society, 2009 , vol. 131, p. 4031 - 4041
反应条件
aluminum oxide in N,N-dimethyl-formamide T=120°C; 10 h; Inert atmosphere;
参考文献
Damodara, Dandu; Arundhathi, Racha; Likhar, Pravin R.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 189 - 198
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=110°C; 12 h;
参考文献
Dobbs
Journal of Organic Chemistry, 2001 , vol. 66, # 2 p. 638 - 641
反应条件
5 Ru/MgO; hydrogen in tetrahydrofuran T=150°C; P=38002.6 Torr; 0.2 h;
参考文献
Journal of Catalysis, , vol. 311, p. 357 - 368
反应条件
1,4-dioxane; copper oxide-chromium oxide T=230°C; P=183877 - 220652 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 63, p. 1563,1568
