4,5-二氯邻苯二甲酸酐合成路线 （共 38 条）
反应条件
aluminium trichloride; sodium chloride T=220°C; Friedel-Crafts reaction; 1.5 h;
参考文献
Hua, Duy H.; Lou, Kaiyan; Havens, Josh; Perchellet, Elisabeth M.; Wang, Yang; Perchellet, Jean-Pierre; Iwamoto, Takeo
Tetrahedron, 2004 , vol. 60, # 45 p. 10155 - 10163
反应条件
1: aluminium chloride
2: concentrated sulfuric acid
View Scheme
参考文献
Barnett; Goodway; Watson
Chemische Berichte, 1933 , vol. 66, p. 1876,1886
反应条件
trimethylsilylazide in toluene
T=80 - 110°C; 37 h;
参考文献
CHIRON CORPORATION
Patent: WO2004/18419 A2, 2004 ;
Location in patent: Page 324 ;
反应条件
sodium acetate in acetic acid
1 h; Heating;
参考文献
Caswell; Guevara; Corley; Martinez; Hollis; Largess; Thornley
Synthesis, 1992 , # 9 p. 823 - 825
反应条件
1: H2O
2: 76.5 percent / 6 h / 160 °C
View Scheme
参考文献
Mazzocchi, P. H.; Wilson, P.; Khachik, F.; Klingler, L.; Minamikawa, S.
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 2981 - 2989
反应条件
acetic acid
0.5 h; Heating;
参考文献
Caswell; Guevara; Corley; Martinez; Hollis; Largess; Thornley
Synthesis, 1992 , # 9 p. 823 - 825
反应条件
1: 91 percent / acetic anhydride, triethylamine / 24 h
View Scheme
参考文献
Lusis, V. K.; Mutsenietse, D. Kh.; Zandersons, A. Z.; Mazheika, I. B.; Dubur, G. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 3 p. 318 - 323
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 3 p. 393 - 398
反应条件
1: 90 percent / AlCl3; NaCl / 1.5 h / 220 °C
2: 82 percent / NaBH4 / methanol / 15 h / 25 °C
View Scheme
参考文献
Hua, Duy H.; Lou, Kaiyan; Havens, Josh; Perchellet, Elisabeth M.; Wang, Yang; Perchellet, Jean-Pierre; Iwamoto, Takeo
Tetrahedron, 2004 , vol. 60, # 45 p. 10155 - 10163
