5-乙酰基噻吩-2-硼酸频那醇酯合成路线 (共 4 条)
反应条件
in tetrahydrofuran
T=40°C; Low pressure;
参考文献
Barcellos, Thiago; Tauber, Katharina; Kroutil, Wolfgang; Andrade, Leandro H.
Tetrahedron Asymmetry, 2011 , vol. 22, # 18-19 p. 1772 - 1777
反应条件
4,4'-di(tert-butyl)-2,2'-dipyridyl; [Ir(μ2-OMe)(1,4-cyclooctadiene)]2 in hexane
T=20°C; 0.5 h;
参考文献
Chotana, Ghayoor A.; Kallepalli, Venkata A.; Maleczka Jr., Robert E.; Smith III, Milton R.
Tetrahedron, 2008 , vol. 64, # 26 p. 6103 - 6114
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran
T=80°C; 18 h; Inert atmosphere;
参考文献
Robbins, Daniel W.; Hartwig, John F.
Organic Letters, 2012 , vol. 14, # 16 p. 4266 - 4269
反应条件
potassium phosphate; (1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane; water
T=40°C; Suzuki-Miyaura cross-coupling; 18 h; Inert atmosphere;
参考文献
Robbins, Daniel W.; Hartwig, John F.
Organic Letters, 2012 , vol. 14, # 16 p. 4266 - 4269