反应条件
1.1: thionyl chloride / 0.33 h / 0 °C / Inert atmosphere
1.2: 15 h / 0 - 22 °C / Inert atmosphere
2.1: caesium carbonate / N,N-dimethyl-formamide / 456 h / Inert atmosphere
3.1: water; lithium hydroxide hydrate / tetrahydrofuran / 189 h / 22 °C / Inert atmosphere
3.2: Inert atmosphere
View Scheme
参考文献
Hardegger, Leo A.; Kuhn, Bernd; Spinnler, Beat; Anselm, Lilli; Ecabert, Robert; Stihle, Martine; Gsell, Bernard; Thoma, Ralf; Diez, Joachim; Benz, Joerg; Plancher, Jean-Marc; Hartmann, Guido; Banner, David W.; Haap, Wolfgang; Diederich, Francois
Angewandte Chemie - International Edition, 2011 , vol. 50, # 1 p. 314 - 318