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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
94242-82-7
合成路线
（共 11 条）
1259299-79-0
→
反应条件
165904-22-3
2-苯基乙基-1-硼酸频哪醇酯
+
94242-82-7
反应条件
(tricyclohexylphosphine)(1,5-cyclooctadiene)pyridineiridium(I) hexafluorophosphate; hydrogen in dichloromethane T=50°C; P=7500.75 Torr; 12 h; chemoselective reaction;
参考文献
Gaziaesmiloviae, Ivana; Casas-Arce, Eva; Roseblade, Stephen J.; Nettekoven, Ulrike; Zanotti-Gerosa, Antonio; Kovacevic, Miroslav; Casar, Zdenko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 4 p. 1014 - 1018
1589-82-8
苄基溴化镁
→
反应条件
94242-82-7
反应条件
1: diethyl ether / -78 - 25 °C 2: H2SO4 3: tetrahydrofuran / -100 - 25 °C View Scheme
参考文献
Priestley; De Lucca, Indawati; Ghavimi, Bahman; Erickson-Viitanen, Susan; Decicco, Carl P.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 21 p. 3199 - 3202
162213-35-6
→
反应条件
94242-82-7
反应条件
1: H2SO4 2: tetrahydrofuran / -100 - 25 °C View Scheme
参考文献
Priestley; De Lucca, Indawati; Ghavimi, Bahman; Erickson-Viitanen, Susan; Decicco, Carl P.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 21 p. 3199 - 3202
2146-67-0
+
87100-28-5
苄基硼酸频哪醇酯
→
反应条件
94242-82-7
反应条件
in tetrahydrofuran T=-100 - 25°C;
参考文献
Priestley; De Lucca, Indawati; Ghavimi, Bahman; Erickson-Viitanen, Susan; Decicco, Carl P.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 21 p. 3199 - 3202
61676-62-8
异丙醇频哪醇硼酸酯
→
反应条件
165904-22-3
2-苯基乙基-1-硼酸频哪醇酯
+
94242-82-7
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C 1.2: 2 h / -78 °C / Inert atmosphere 1.3: -78 - 20 °C / Inert atmosphere 2.1: Schwartz's reagent / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: (tricyclohexylphosphine)(1,5-cyclooctadiene)pyridineiridium(I) hexafluorophosphate; hydrogen / dichloromethane / 12 h / 50 °C / 7500.75 Torr View Scheme
参考文献
Gaziaesmiloviae, Ivana; Casas-Arce, Eva; Roseblade, Stephen J.; Nettekoven, Ulrike; Zanotti-Gerosa, Antonio; Kovacevic, Miroslav; Casar, Zdenko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 4 p. 1014 - 1018
536-74-3
苯乙炔
→
反应条件
165904-22-3
2-苯基乙基-1-硼酸频哪醇酯
+
94242-82-7
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C 1.2: 2 h / -78 °C / Inert atmosphere 1.3: -78 - 20 °C / Inert atmosphere 2.1: Schwartz's reagent / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: (tricyclohexylphosphine)(1,5-cyclooctadiene)pyridineiridium(I) hexafluorophosphate; hydrogen / dichloromethane / 12 h / 50 °C / 7500.75 Torr View Scheme
参考文献
Gaziaesmiloviae, Ivana; Casas-Arce, Eva; Roseblade, Stephen J.; Nettekoven, Ulrike; Zanotti-Gerosa, Antonio; Kovacevic, Miroslav; Casar, Zdenko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 4 p. 1014 - 1018
159087-45-3
2-苯基-1-乙炔硼酸频那醇酯
→
反应条件
165904-22-3
2-苯基乙基-1-硼酸频哪醇酯
+
94242-82-7
反应条件
1.1: Schwartz's reagent / dichloromethane / 1 h / 20 °C / Inert atmosphere 1.2: Inert atmosphere 2.1: (tricyclohexylphosphine)(1,5-cyclooctadiene)pyridineiridium(I) hexafluorophosphate; hydrogen / dichloromethane / 12 h / 50 °C / 7500.75 Torr View Scheme
参考文献
Gaziaesmiloviae, Ivana; Casas-Arce, Eva; Roseblade, Stephen J.; Nettekoven, Ulrike; Zanotti-Gerosa, Antonio; Kovacevic, Miroslav; Casar, Zdenko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 4 p. 1014 - 1018
83622-41-7
+
6921-34-2
苄基氯化镁
→
反应条件
94242-82-7
反应条件
in not given by procedure of Sadhu, K. M.; Matteson, D. S.; Hurst, G. D.; Kurosky, J. M. Organometallics 1984, 3, 804-806; elem. anal.;
参考文献
Matteson, Donald S.; Wilson, John W.
Organometallics, 1985 , vol. 4, p. 1690 - 1692
1259299-79-0
+
1333-74-0
氢气
→
反应条件
165904-22-3
2-苯基乙基-1-硼酸频哪醇酯
+
94242-82-7
反应条件
暂无反应条件数据
参考文献
Gazic Smilovic, Ivana; Casas-Arce, Eva; Roseblade, Stephen J.; Nettekoven, Ulrike; Zanotti-Gerosa, Antonio; et al.
Angew. Chem., 2012 , vol. 51, p. 1014 - 1018
Angewandte Chemie, 2012 , vol. 124, p. 1038 - 1042
76-09-5
频哪醇
→
反应条件
94242-82-7
反应条件
1: tetrahydrofuran / -100 - 25 °C View Scheme
参考文献
Priestley; De Lucca, Indawati; Ghavimi, Bahman; Erickson-Viitanen, Susan; Decicco, Carl P.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 21 p. 3199 - 3202
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