反应条件
1: 99 percent
2: 1.) O3; 2.) MeS / 1.) CH2Cl2, -78 deg C
3: 95 percent / H2 / PtO2 / ethanol
4: 85 percent / Me3SiI / acetonitrile / 16 h / Ambient temperature
5: 25 percent
6: 1.) KHSO4; 2.) KI, (i-Pr)2NEt / 1.) 170 deg C; 2.) CH3CN
View Scheme
参考文献
Holmes, Andrew B.; Russell, Keith; Stern, Edward S.; Stubbs, Michael E.; Wellard, Nicolas K.
Tetrahedron Letters, 1984 , vol. 25, # 37 p. 4163 - 4166
