4-溴-6-氯-7-氮杂吲哚合成路线 (共 2 条)
反应条件
1: With methanesulfonyl chloride in N,N-dimethyl-formamide T=75°C; 1 h; 2: With sodium hydroxide in water; N,N-dimethyl-formamide T=5 - 20°C; pH=7; 3 h;
参考文献
DHANAK, Dashyant; Newlander, Kenneth Allen
Patent: US2007/149561 A1, 2007 ;
Location in patent: Page/Page column 90-91 ;
US 20070149561 A1
反应条件
1: 3-chloro-benzenecarboperoxoic acid / diethyl ether / 3.33 h / 0 - 20 °C 2: methanesulfonyl chloride / N,N-dimethyl-formamide / 50 - 75 °C View Scheme
参考文献
WO2012/170752 A1, ;
WO 2012/170752 A1