反应条件
in pentane
byproducts: ethyl chloride; argon atmosphere; BCl3 soln. addn. to Si-compd. soln. (stirring, cooling to -50°C), light fraction driving off (vac.) into trap cooled with solid CO2; residue distn.; elem. anal.;
参考文献
Ponomarev, S. V.; Nikolaeva, S. N.; Molchanova, G. N.; Kostyuk, A. S.; Grishin, Yu. K.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1620 - 1623
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 1817 - 1821
