hydrogen; palladium on activated charcoal in hexane T=20°C; P=3206.4 Torr; 3 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209320', constants.ctx, '0')">sodium azide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605365', constants.ctx, '0')">N,N-dimethyl-formamide</a> <br />T=85&deg;C;&nbsp;4&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1.1: Mg; iodine / tetrahydrofuran<br />1.2: tetrahydrofuran / 72 h / 65 - 70 &deg;C<br />2.1: triethylamine / tetrahydrofuran / 0.25 h / 20 &deg;C<br />3.1: 92 percent / sodium azide / dimethylformamide / 4 h / 85 &deg;C<br /> <br /> &nbsp;