1-(三氟乙酰基)-2-哌啶酮合成路线 （共 2 条）
反应条件
in toluene
T=25°C; 0.5 h;
参考文献
Yue, Tai-Yuen; Nugent, William A.
Journal of the American Chemical Society, 2002 , vol. 124, # 46 p. 13692 - 13693
反应条件
1: potassium tert-butylate / tert-butyl alcohol; tetrahydrofuran / 1 h / 60 °C / |Large scale
2: palladium 10 on activated carbon; hydrogen / methanol / 6 h / 25 °C / 3604.44 Torr / |Large scale
3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 15 - 30 °C / |Large scale
View Scheme
参考文献
Yue, Tai-Yuen; McLeod, Douglas D.; Albertson, Kevin B.; Beck, Steven R.; Deerberg, Joerg; Fortunak, Joseph M.; Nugent, William A.; Radesca, Lilian A.; Tang, Liya; Xiang, Cathie Dong
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 262 - 271
