1: 3-(butyltellanyl)propan-1-ol With n-butyllithium in tetrahydrofuran; hexane
cooling;
2: in tetrahydrofuran; hexane
T=-70°C; 1 h;
3: cyclohexenon in tetrahydrofuran; hexane
T=-78 - 20°C; Further stages.;
参考文献
Dos Santos, Alcindo A.; Princival, Jefferson L.; Comasseto, Joao V.; de Barros, Simone M.G.; Neto, Jose E. Brainer
Tetrahedron, 2007 , vol. 63, # 24 p. 5167 - 5172