2,2'-亚乙基双(2-甲基-1,3-二氧戊环)合成路线 (共 19 条)
反应条件
1: 95 percent / potassium hydroxide / H2O / Heating
2: 95 percent / potassium hydroxide / methanol / Heating; electrolysis
View Scheme
参考文献
Einhorn, Jacques; Soulier, Jean-Louis; Bacquet Cathy; Lelandais Daniel
Canadian Journal of Chemistry, 1983 , vol. 61, p. 584 - 587
反应条件
1: 50 percent Turnov. / Na2S2O8, FeSO4*7H2O / H2O / 6 h / 80 - 85 °C
2: 4.0 g / pyridinium p-toluene sulfonate (PPTS) / benzene / Heating
View Scheme
参考文献
Troyanskii, E.I.; Mizintsev, V. V.; Lazareva, M. I.; Demchuk, D. V.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 91 p. 1879 - 1884
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 9 p. 2044 - 2049
反应条件
in methanol
electrolysis;
参考文献
Daubie, Christophe; Bacquet-Einhorn, Cathy; Lelandais, Daniel
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1552 - 1554
反应条件
in methanol
electrolysis;
参考文献
Daubie, Christophe; Bacquet-Einhorn, Cathy; Lelandais, Daniel
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1552 - 1554
反应条件
in methanol
electrolysis;
参考文献
Daubie, Christophe; Bacquet-Einhorn, Cathy; Lelandais, Daniel
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1552 - 1554
反应条件
in methanol
electrolysis;
参考文献
Daubie, Christophe; Bacquet-Einhorn, Cathy; Lelandais, Daniel
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1552 - 1554
反应条件
in methanol
electrolysis;
参考文献
Daubie, Christophe; Bacquet-Einhorn, Cathy; Lelandais, Daniel
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1552 - 1554
反应条件
diethyl ether; benzene
Anschliessend Behandeln mit Heptanal und Behandeln des Reaktionsgemisches mit wss. Ammoniumchlorid.;
参考文献
Theus et al.
Helvetica Chimica Acta, 1955 , vol. 38, p. 239,249
反应条件
in methanol
anodic oxidation; Mechanism;
参考文献
Lelandais, Daniel; Bacquet, Cathy; Einhorn, Jacques
Tetrahedron, 1981 , vol. 37, # 18 p. 3131 - 3134