3-苄氧基-2-甲酰基吡啶合成路线 （共 5 条）
反应条件
manganese(IV) oxide in 1,4-dioxane T=80°C; 2 h;
参考文献
Pfizer Inc
Patent: US2008/85887 A1, 2008 ;
Location in patent: Page/Page column 23 ;
US 20080085887 A1
反应条件
1.1: NaOEt / ethanol / 1 h / 20 °C 1.2: 39 percent / dimethylsulfoxide / 12 h / 20 °C 2.1: 84 percent / SeO2 / dioxane / Heating View Scheme
参考文献
Tetrahedron, , vol. 61, # 3 p. 643 - 655
反应条件
1: 1.) EtONa / 1.) ethanol, RT, 1 h, 2.) DMSO, RT, overnight 2: 95 percent / MnO2 / 1,2-dimethoxy-ethane / 1 h / 100 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 26, # 4 p. 455 - 460
反应条件
1: 66 percent / KOH / ethanol / 24 h / Heating 2: 73 percent / MnO2 / CHCl3 / 1.33 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 20 p. 4431 - 4447
反应条件
1: potassium hydroxide / ethanol / 24 h / 20 °C / |Reflux 2: manganese(IV) oxide / chloroform / 1.5 h / |Reflux View Scheme
