5,8-二溴-2,3-二苯基喹喔啉合成路线 （共 6 条）
反应条件
1: CuI; NEt3 / (Ph3P)2PdCl2 / tetrahydrofuran 2: K2CO3 View Scheme
参考文献
Bangcuyo, Carlito G.; Ellsworth, Joe M.; Evans, Una; Myrick, Michael L.; Bunz, Uwe H.F.
Macromolecules, 2003 , vol. 36, # 3 p. 546 - 548
反应条件
toluene-4-sulfonic acid in chloroform
12 h; Heating;
参考文献
Chen, Chien-Tien; Wei, Yi; Lin, Jin-Sheng; Moturu, Murthy V. R. K.; Chao, Wei-San; Tao, Yu-Tai; Chien, Chin-Hsiung
Journal of the American Chemical Society, 2006 , vol. 128, # 34 p. 10992 - 10993
反应条件
in acetic acid; toluene
Reflux;
参考文献
Chang, Dong Wook; Lee, Hyo Joong; Kim, Jong H.; Park, Soo Young; Park, Su-Moon; Dai, Liming; Baek, Jong-Beom
Organic Letters, 2011 , vol. 13, # 15 p. 3880 - 3883
反应条件
1: 87 percent / NaBH4 / ethanol / 20 h / 0 - 20 °C
2: 70 percent / ethanol / 1 h / Heating
View Scheme
参考文献
Edelmann, Michael J.; Raimundo, Jean-Manuel; Utesch, Nils F.; Diederich, Francois; Boudon, Corinne; Gisselbrecht, Jean-Paul; Gross, Maurice
Helvetica Chimica Acta, 2002 , vol. 85, # 7 p. 2195 - 2213
反应条件
1: 88 percent / Br2; HBr / H2O / 2 h / Heating
2: 87 percent / NaBH4 / ethanol / 20 h / 0 - 20 °C
3: 70 percent / ethanol / 1 h / Heating
View Scheme
参考文献
Edelmann, Michael J.; Raimundo, Jean-Manuel; Utesch, Nils F.; Diederich, Francois; Boudon, Corinne; Gisselbrecht, Jean-Paul; Gross, Maurice
Helvetica Chimica Acta, 2002 , vol. 85, # 7 p. 2195 - 2213
反应条件
1: zinc; acetic acid / 60 - 70 °C
2: concentrated alcohol
View Scheme
参考文献
Calhane; Wheeler
American Chemical Journal, 1899 , vol. 22, p. 452
