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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7-碘-1H-吲唑
合成路线
（共 8 条）
21443-96-9
7-氨基吲唑
→
反应条件
945761-94-4
7-碘-1H-吲唑
反应条件
hydrogenchloride; sulfuric acid; sodium nitrite; potassium iodide T=0°C;
参考文献
Cottyn, Betty; Acher, Francine; Ramassamy, Booma; Alvey, Luke; Lepoivre, Michel; Frapart, Yves; Stuehr, Dennis; Mansuy, Daniel; Boucher, Jean-Luc; Vichard, Dominique
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 11 p. 5962 - 5973
570-24-1
2-甲基-6-硝基苯胺
→
反应条件
945761-94-4
7-碘-1H-吲唑
反应条件
1: 98 percent / aq. NaNO2; glacial acetic acid / 0.33 h 2: 75 percent / NH4(+)HCOO(-); H2 / Pd/C / ethanol 3: 71 percent / HCl; H2SO4; NaNO2 / KI / 0 °C View Scheme
参考文献
Synlett, , # 8 p. 1203 - 1206
2942-42-9
7-硝基吲唑
→
反应条件
945761-94-4
7-碘-1H-吲唑
反应条件
1: 75 percent / NH4(+)HCOO(-); H2 / Pd/C / ethanol 2: 71 percent / HCl; H2SO4; NaNO2 / KI / 0 °C View Scheme
参考文献
Synlett, , # 8 p. 1203 - 1206
945761-94-4
7-碘-1H-吲唑
→
反应条件
945762-00-5
7-氰基-3-溴-1H-吲唑
反应条件
1: 79 percent / NBS; NaOH / dimethylformamide / 48 h / 20 °C 2: 53 percent / dppf; Zn / Pd2(dba)3 / N,N-dimethyl-acetamide / 5 h / Heating View Scheme
参考文献
Cottyn, Betty; Vichard, Dominique; Terrier, Francois; Nioche, Pierre; Raman
Synlett, 2007 , # 8 p. 1203 - 1206
945761-94-4
7-碘-1H-吲唑
+
557-21-1
氰化锌
→
反应条件
256228-64-5
7-氰基-1H-吲唑
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; zinc; tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl acetamide Heating;
参考文献
Cottyn, Betty; Vichard, Dominique; Terrier, Francois; Nioche, Pierre; Raman
Synlett, 2007 , # 8 p. 1203 - 1206
945761-94-4
7-碘-1H-吲唑
→
反应条件
945761-95-5
3-溴-7-碘-1H-吲唑
反应条件
sodium hydroxide; N-bromosuccinmide in N,N-dimethyl-formamide T=20°C; 48 h;
参考文献
Cottyn, Betty; Acher, Francine; Ramassamy, Booma; Alvey, Luke; Lepoivre, Michel; Frapart, Yves; Stuehr, Dennis; Mansuy, Daniel; Boucher, Jean-Luc; Vichard, Dominique
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 11 p. 5962 - 5973
945761-94-4
7-碘-1H-吲唑
+
1066-54-2
三甲基乙炔基硅
→
反应条件
945761-98-8
7-三甲基硅基炔基-1H-吲唑
反应条件
copper(l) iodide; triethylamine; triphenylphosphine in acetonitrile T=20°C; 6 h;
参考文献
Cottyn, Betty; Acher, Francine; Ramassamy, Booma; Alvey, Luke; Lepoivre, Michel; Frapart, Yves; Stuehr, Dennis; Mansuy, Daniel; Boucher, Jean-Luc; Vichard, Dominique
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 11 p. 5962 - 5973
945761-94-4
7-碘-1H-吲唑
→
反应条件
945761-99-9
反应条件
1: 70 percent / Et3N; PPh3; CuI / acetonitrile / 6 h / 20 °C View Scheme
参考文献
Cottyn, Betty; Vichard, Dominique; Terrier, Francois; Nioche, Pierre; Raman
Synlett, 2007 , # 8 p. 1203 - 1206
