(S)-(+)-(2-丁烯酰)-2,10-樟脑磺内酰胺合成路线 （共 7 条）
反应条件
sodium hydride in toluene T=20°C;
参考文献
Liang, Bo; Carroll, Patrick J.; Joullie, Madeleine M.
Organic Letters, 2000 , vol. 2, # 26 p. 4157 - 4160
反应条件
copper dichloride in toluene 16 h; Heating;
参考文献
Thom; Kocienski
Synthesis, 1992 , # 6 p. 582 - 586
反应条件
1: SOCl2 2: NH3 / dioxane; H2O 3: 100 percent / NaBH4 / methanol; H2O 4: 90 percent / NaH / toluene; various solvent(s) / 20 °C View Scheme
参考文献
Organic Letters, , vol. 2, # 26 p. 4157 - 4160
反应条件
1: NH3 / dioxane; H2O 2: 100 percent / NaBH4 / methanol; H2O 3: 90 percent / NaH / toluene; various solvent(s) / 20 °C View Scheme
参考文献
Organic Letters, , vol. 2, # 26 p. 4157 - 4160
反应条件
1: 100 percent / NaBH4 / methanol; H2O 2: 90 percent / NaH / toluene; various solvent(s) / 20 °C View Scheme
参考文献
Organic Letters, , vol. 2, # 26 p. 4157 - 4160
反应条件
1: 91 percent / triethylamine / benzene; acetonitrile / 1.5 h / Ambient temperature 2: 86 percent / anhydr. CuCl2 / toluene / 16 h / Heating View Scheme
参考文献
Synthesis, , # 6 p. 582 - 586
反应条件
1: 99.3 percent / NaOMe / methanol / 64 h / Ambient temperature 2: 1.) LiAlH4; 2.) 1N aq. HCl / 1.) THF, 0 deg C, 2.) r.t., 1 h 3: 88 percent / NaH / toluene / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 42, # 14 p. 4035 - 4044
