3-乙基-4-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)苯酚合成路线 (共 3 条)
反应条件
sodium periodate; ammonium acetate; water in acetone T=20°C; 68 h;
参考文献
US2008/96921 A1, ;
Page/Page column 82 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium acetate in polyethylene glycol 600
T=90°C; 10 h; Inert atmosphere;
参考文献
Lu, Jie; Guan, Zhong-Zhi; Gao, Jian-Wu; Zhang, Zhan-Hui
Applied Organometallic Chemistry, 2011 , vol. 25, # 7 p. 537 - 541
反应条件
potassium acetate; tris-(dibenzylideneacetone)dipalladium(0); tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=20 - 80°C; 20.5 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2007/140183 A1, 2007 ;
Location in patent: Page/Page column 35-36 ;