反应条件
1.1: 92 percent / palladium(II) acetate; 1,1'-bis(diphenylphosphino)ferrocene; lithium chloride / triethylamine; triethylborane / tetrahydrofuran; hexane / 24 h / 50 °C
2.1: 88 percent / NaBH4 / ethanol / 16 h / 20 °C
3.1: NaH / dimethylformamide / 3 h / 20 °C
3.2: 27 percent / dimethylformamide / 24 h / 20 °C
View Scheme
参考文献
Kimura, Masanari; Ezoe, Akihiro; Mori, Masahiko; Tamaru, Yoshinao
Journal of the American Chemical Society, 2005 , vol. 127, # 1 p. 201 - 209