n-butyllithium; magnesium bromide in tetrahydrofuran; diethyl ether 1.) -78 deg C, 10 min, 2a.) -78 deg C, 15 min, 2b.) -78 deg C to 25 deg C, 50 min;

n-butyllithium; magnesium bromide in tetrahydrofuran; diethyl ether 1.) -78 deg C, 10 min, 2a.) -78 deg C, 15 min, 2b.) -78 deg C to 25 deg C, 50 min;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '4154566', constants.ctx, '0')">sodium carbonate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '608317', constants.ctx, '0')">3-chloro-benzenecarboperoxoic acid</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0&deg;C;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: Br₂, acetic acid<br />2: 1.) n-BuLi / 1.) THF, 0 deg C, 1 h, 2.) benzene, RT, 2 h<br />3: 80 percent / Na₂CO₃, m-chloroperbenzoic acid / CH₂Cl₂ / 0 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 95 percent / benzene / Heating<br />2: 1.) n-BuLi / 1.) THF, 0 deg C, 1 h, 2.) benzene, RT, 2 h<br />3: 80 percent / Na₂CO₃, m-chloroperbenzoic acid / CH₂Cl₂ / 0 &deg;C<br /> <br /> &nbsp;