S-(11-溴十一烷基)硫代乙酸酯合成路线 （共 6 条）
反应条件
acetyl chloride in methanol T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Lim, Jongmin; Yang, Hyunseung; Paek, Kwanyeol; Cho, Chul-Hee; Kim, Seyong; Bang, Joona; Kim, Bumjoon J.
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3464 - 3474
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
T=25°C; 1 h; Inert atmosphere;
参考文献
Sureshkumar, Gopalsamy; Hotha, Srinivas
Glycoconjugate Journal, 2012 , vol. 29, # 4 p. 221 - 230
反应条件
2,2'-azo-bisisobutyronitrile in toluene
4 h; Inert atmosphereReflux;
参考文献
Lim, Jongmin; Yang, Hyunseung; Paek, Kwanyeol; Cho, Chul-Hee; Kim, Seyong; Bang, Joona; Kim, Bumjoon J.
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 16 p. 3464 - 3474
反应条件
2,2'-azo-bisisobutyronitrile in toluene
2 h; Heating / reflux;
参考文献
THE UNIVERSITY OF NORTH CAROLINA AT CHAPEL HILL
Patent: WO2006/128121 A2, 2006 ;
Location in patent: Page/Page column 57; Sheet 11/36 ;
反应条件
1: 2,2'-azo-bisisobutyronitrile / 1,4-dioxane / 24 h / 25 - 75 °C / Inert atmosphere
2: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / 25 °C / Inert atmosphere
View Scheme
参考文献
Sureshkumar, Gopalsamy; Hotha, Srinivas
Glycoconjugate Journal, 2012 , vol. 29, # 4 p. 221 - 230
反应条件
sodium azide in N,N-dimethyl-formamide
T=25°C; 20 h; Inert atmosphere;
参考文献
Sureshkumar, Gopalsamy; Hotha, Srinivas
Glycoconjugate Journal, 2012 , vol. 29, # 4 p. 221 - 230
