1-[双(4-氯苯基)甲基]-3-[2-(2,4-二氯苯基)-2-(2,4-二氯苄氧基)乙基]-1H-咪唑氯化物合成路线 （共 4 条）
参考文献
IMPERIAL COLLEGE INNOVATIONS LTD
Patent: WO2005/23744 A2, 2005 ;
Location in patent: Page/Page column 16; 20-21 ;
反应条件
perchloric acid in water
T=90°C; 4 h; Yield given. Yields of byproduct given;
参考文献
Katsu; Ono; Tasaka; Fujita
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 4185 - 4188
反应条件
1: SOCl2 / 0.5 h / Heating
2: 73 percent / methanol / 168 h / Ambient temperature
3: 20percent perchloric acid / H2O / 4 h / 90 °C
View Scheme
参考文献
Katsu; Ono; Tasaka; Fujita
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 4185 - 4188
反应条件
1: 73 percent / methanol / 168 h / Ambient temperature
2: 20percent perchloric acid / H2O / 4 h / 90 °C
View Scheme
参考文献
Katsu; Ono; Tasaka; Fujita
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 4185 - 4188
