1: 2) acid
2: 93 percent / (EtO)3P / benzene / 4.5 h / Ambient temperature
View Scheme
参考文献
Hickey, Deirdre M. B.; MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Chemical Communications, 1984 , # 12 p. 776 - 777
1: 1.) 1.6 M butyl-lithium / 1.) THF, -100 deg C, 15 min
2: 36 percent / NaOMe / methanol
3: 62 percent / 6 M HCl / tetrahydrofuran; H2O / 22 h / Ambient temperature
4: 93 percent / triethyl phosphite / benzene / 4.5 h / Ambient temperature
View Scheme
参考文献
Hickey, Deirdre M. B.; MacKenzie, A. Roderick; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 921 - 926