2-(1,1-二甲基丙基)-6-(二苯基膦)吡啶合成路线 （共 4 条）
反应条件
in tetrahydrofuran
T=0°C; 1 h;
参考文献
Hintermann, Lukas; Dang, Tuan Thanh; Labonne, Aurelie.; Kribber, Thomas; Xiao, Li; Naumov, Pance
Chemistry - A European Journal, 2009 , vol. 15, # 29 p. 7167 - 7179
反应条件
1: bis-diphenylphosphine With n-butyllithium in tetrahydrofuran; hexane
T=20°C; 0.5 h; Inert atmosphere;
2: 2-chloro-6-tert-amylpyridine in tetrahydrofuran; hexane
T=0 - 20°C; Inert atmosphere;
参考文献
Hintermann, Lukas; Dang, Tuan Thanh; Labonne, Aurelie.; Kribber, Thomas; Xiao, Li; Naumov, Pance
Chemistry - A European Journal, 2009 , vol. 15, # 29 p. 7167 - 7179
反应条件
dimethylsulfide in dichloromethane
T=20°C; 96 h; Inert atmosphereSchlenk technique;
参考文献
Tomas-Mendivil, Eder; Garcia-Alvarez, Rocio; Garcia-Garrido, Sergio E.; Diez, Josefina; Crochet, Pascale; Cadierno, Victorio
Journal of Organometallic Chemistry, 2013 , vol. 727, p. 1 - 9
反应条件
dimethylsulfide in dichloromethane
T=20°C; 96 h; Inert atmosphereSchlenk technique;
参考文献
Tomas-Mendivil, Eder; Garcia-Alvarez, Rocio; Garcia-Garrido, Sergio E.; Diez, Josefina; Crochet, Pascale; Cadierno, Victorio
Journal of Organometallic Chemistry, 2013 , vol. 727, p. 1 - 9
