2-((三甲基甲硅烷基)乙炔)吡啶-3-胺合成路线 （共 4 条）
反应条件
potassium tert-butylate in 1-methyl-pyrrolidin-2-one T=20°C; 5 h;
参考文献
Sun, Li-Ping; Wang, Jin-Xin
Synthetic Communications, 2007 , vol. 37, # 13 p. 2187 - 2193
反应条件
ammonium chloride; tin(ll) chloride in ethanol
T=60°C; 4 h;
参考文献
Sun, Li-Ping; Wang, Jin-Xin
Synthetic Communications, 2007 , vol. 37, # 13 p. 2187 - 2193
反应条件
1: 50 percent / triethylamine; CuI / Pd(PPh3)4 / acetonitrile / 4 h / 20 °C
2: 60 percent / tin(II) chloride dihydrate; NH4Cl / ethanol / 4 h / 60 °C
View Scheme
参考文献
Sun, Li-Ping; Wang, Jin-Xin
Synthetic Communications, 2007 , vol. 37, # 13 p. 2187 - 2193
反应条件
1: 50 percent / triethylamine; CuI / Pd(PPh3)4 / acetonitrile / 4 h / 20 °C
2: 60 percent / tin(II) chloride dihydrate; NH4Cl / ethanol / 4 h / 60 °C
View Scheme
参考文献
Sun, Li-Ping; Wang, Jin-Xin
Synthetic Communications, 2007 , vol. 37, # 13 p. 2187 - 2193
