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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-苯基吲哚
合成路线
（共 442 条）
615-43-0
2-碘苯胺
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
反应条件
1: 2-iodo aniline; polystyrene sulfonyl chloride With pyridine in dichloromethane T=50°C; Solid phase reaction; condensation; 18 h; 2: phenylacetylene With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in N,N-dimethyl-formamide T=70°C; Solid phase reaction; cyclization; 6 h; 3: With tetrabutyl ammonium fluoride in tetrahydrofuran T=70°C; Substitution; 5 h; Further stages.;
参考文献
Organic Letters, , vol. 2, # 1 p. 89 - 92
116547-92-3
+
536-74-3
苯乙炔
→
反应条件
948-65-2
2-苯基吲哚
反应条件
copper(l) iodide; palladium; triphenylphosphine; aluminum oxide; potassium fluoride Sonogashira coupling-cyclization; 0.05 h; microwave irradiation (100 percent power);
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
98-86-2
苯乙酮
→
反应条件
948-65-2
2-苯基吲哚
反应条件
1: 0.5 h / 100 °C 2: ZnCl2 / N,N-dimethyl-acetamide / 12 h / 170 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 41, # 8 p. 985 - 990
103529-16-4
2-[(三甲基甲硅烷基)乙炔基]苯胺
→
反应条件
948-65-2
2-苯基吲哚
反应条件
1: 0.940 g / KF/Al2O3 / 0.07 h / microwave irradiation (30 percent power) 2: 88 percent / Et3N / tetrahydrofuran / -15 - 20 °C 3: PPh3; CuI; Pd / KF/Al2O3 / microwave irradiation View Scheme
参考文献
Tetrahedron, , vol. 57, # 38 p. 8017 - 8028
120-72-9
吲哚
+
108-86-1
溴代苯
→
反应条件
16096-33-6
1-苯基-1H-吲哚
+
948-65-2
2-苯基吲哚
+
1504-16-1
3-苯基-1H-吲哚
反应条件
potassium carbonate; triphenylphosphine; palladium diacetate in toluene T=110°C; 24 h; Product distribution; Further Variations:Reaction partnersReagentsSolventsTemperatures;
参考文献
Bellina, Fabio; Benelli, Francesca; Rossi, Renzo
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5529 - 5535
1201632-48-5
→
反应条件
948-65-2
2-苯基吲哚
反应条件
1: With trifluorormethanesulfonic acid in 1,2-dichloro-ethane Reflux; 2: With water; sodium hydrogencarbonate in ethyl acetate; 1,2-dichloro-ethane
参考文献
Wang, Honggen; Liu, Lanying; Wang, Yong; Peng, Changlan; Zhang, Jiancun; Zhu, Qiang
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6841 - 6843
→
反应条件
948-65-2
2-苯基吲哚
反应条件
1: With palladium diacetate; dimethyl sulfoxide; trifluoroacetic acid T=90°C; 24 h; 2: With iron T=90°C; 2 h;
参考文献
Synlett, , vol. 23, # 17 p. 2511 - 2515,5
Synlett, , vol. 23, # 17 p. 2511 - 2515
4212-33-3
→
反应条件
948-65-2
2-苯基吲哚
反应条件
sodium acetate; iron; acetic acid in ethanol; water 2 h; Inert atmosphereReflux;
参考文献
Hering, Thea; Hari, Durga Prasad; Koenig, Burkhard
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10347 - 10352
74497-02-2
+
70-11-1
2-溴苯乙酮
→
反应条件
948-65-2
2-苯基吲哚
反应条件
T=150°C; Bischler-Moehlau reaction; P=1034.32 Torr; 0.166667 h; Microwave irradiationNeat (no solvent); regioselective reaction;
参考文献
Vara, Yosu; Aldaba, Eneko; Arrieta, Ana; Pizarro, Jose L.; Arriortua, Maria I.; Cossio, Fernando P.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 10 p. 1763 - 1772
95578-13-5
→
反应条件
948-65-2
2-苯基吲哚
反应条件
T=600°C; P=0.01 Torr;
参考文献
Fishwick; Randles; Storr; Manley
Tetrahedron Letters, 1985 , vol. 26, # 25 p. 3053 - 3056
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