反应条件
1: 79 percent / MCPBA / diethyl ether / 1 h / -20 °C 2: 1) n-BuLi / 1) THF, DMF, -70 deg C, 20 min 2) 1h 3: NaOEt / tetrahydrofuran / 10 °C 4: 85 percent / HSO3F / various solvent(s) / -90 °C 5: 81 percent / CrO3, pyridine / CH2Cl2 / 0.5 h / 25 °C 6: 95 percent / 8.5percent methanolic KOH / 2 h / 25 °C View Scheme
参考文献
Moiseenkov, A. M.; Veselovskii, V. V.; Dragan, V. A.; Stashina, G. A.; Zhulin, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 11.2 p. 2394 - 2397
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 11 p. 2607 - 2610
