1: 420 g / NaH / toluene; paraffin / 45 - 50 °C
2: dicyclohexylcarbodiimide / CH2Cl2 / 3 h
3: 1) NaH, 2) 10percent ethanolic KOH / 1) toluene, mineral oil, 2) reflux, 4 h
4: AcCl / CH2Cl2 / 3 h
View Scheme
参考文献
Glaze, Alan P.; Heller, Harry G.; Whittall, John
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 4 p. 591 - 594
1: 1) NaH, 2) 10percent ethanolic KOH / 1) toluene, mineral oil, 2) reflux, 4 h
2: AcCl / CH2Cl2 / 3 h
View Scheme
参考文献
Glaze, Alan P.; Heller, Harry G.; Whittall, John
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 4 p. 591 - 594
in toluene
Irradiationvariation of wavelength, other temperatures; Quantum yield;
参考文献
Glaze, Alan P.; Heller, Harry G.; Whittall, John
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 4 p. 591 - 594
