2-氨基-5-甲基苯硼酸频那醇酯合成路线 （共 4 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in 1,4-dioxane
T=120°C; 12 h; Inert atmosphere;
参考文献
Zhou, Fei; Driver, Tom G.
Organic Letters, 2014 , vol. 16, # 11 p. 2916 - 2919
反应条件
N(CH2CH3)3; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane
(Ar); addn. of triethylamine, palladium compd. and borane deriv. to dioxane soln. of aniline deriv., heating at 100°C for 5 h; cooling to room temp., filtration through celite with eluting by ethyl acetate, evapn., chromy. (silica gel, hexane/ethyl acetate (9/1 to 6/4)),NMR and MS;
参考文献
Soto, Sara; Vaz, Esther; Dell'Aversana, Carmela; Alvarez, Rosana; Altucci, Lucia; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 10 p. 2101 - 2112
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium acetate; tri-cyclo-hexyl-phosphine in 1,4-dioxane
T=80°C; 16 h; Inert atmosphere;
参考文献
Agarwal, Piyush K.; Saifuddin, Mohammad; Kundu, Bijoy
Tetrahedron, 2010 , vol. 66, # 4 p. 862 - 870
反应条件
1: With potassium hydroxide; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in toluene
T=20°C; 24 h; Inert atmosphere;
2: With palladium 10 on activated carbon in toluene
4 h; Reflux; regiospecific reaction;
参考文献
Horn, Joachim; Marsden, Stephen P.; Nelson, Adam; House, David; Weingarten, Gordon G.
Organic Letters, 2008 , vol. 10, # 18 p. 4117 - 4120
